Hi Ben, all,
It's a good thought experiment, but definitely not that simple. Both  the
glasswork and achieving the degree of vacuum required are way out of 
reach of
most experimenters. A hard enough vacuum for a hot cathode  vacuum 
rectifier is
very difficult to reach and requires much more  than just a good 
mechanical
two stage rotary vane pump. Even the vacuum level  used in making neon and
fluorescent tubes is no where good enough for making  electron vacuum 
tubes. And,
while it might provide some rectifying action, it  would likely produce 
some
low energy x-rays too.
That said, if your real goal is to learn something, then by all means go
ahead and try it. (Google "The Bell Jar" magazine for instructions on how 
to
make your own high vacuum pumping systems) I'll even be glad to assist if 
I can.
Even if it doesn't work the first time, you'll learn a lot in the process
and you may come up with a better idea that will.
Tony Greer
**************
In a message dated 8/31/2008 9:31:51 A.M. Central Daylight Time,
bsneath@xxxxxxxxxxxxxxxx writes:
What about building a rectifier from scratch out of a fluro tube? A 4' 
long
tube should hold off a megavolt or two... It would be a fairly simple task
to remove one of the filaments and replace it with a anode plate, then 
pump
it down to a hard vacuum (or abouts). Why go solid state? Although i
cant  imagine what the response time on something like that would be... 
just
a  thought...
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